Friedel–Crafts Acylation

01Friedel–Crafts Acylation

Acylation reaction

This section covers the reagents, conditions, products and synthetic importance of Friedel–Crafts acylation.

Introducing an acyl group

During Friedel–Crafts acylation, benzene undergoes electrophilic substitution and gains an acyl substituent in place of a ring hydrogen. For the acyl chlorides considered here, this substituent contains a carbonyl group bonded to an alkyl group.

Benzene reacts with an acyl chloride, RCOCl\ce{RCOCl}, using anhydrous aluminium chloride, AlClX3\ce{AlCl3}. Changing the alkyl group RR in the acyl chloride changes the acyl group introduced onto the aromatic ring.

Feature Friedel–Crafts acylation
Organic reagent Acyl chloride, RCOCl\ce{RCOCl}
Catalyst Anhydrous AlClX3\ce{AlCl3}
Conditions Heat under reflux, about 50C50^\circ\mathrm{C}
Electrophile Acylium ion, RCOX+\ce{RCO+}
Reaction type Electrophilic substitution

Example: ethanoylation of benzene

With ethanoyl chloride as the acyl chloride, one ring hydrogen is replaced by an ethanoyl group. The products are phenylethanone and hydrogen chloride.

Ethanoyl chloride

Phenylethanone

CX6HX6+CHX3COClCX6HX5COCHX3+HCl\ce{C6H6 + CH3COCl -> C6H5COCH3 + HCl}

The product contains a carbonyl-containing side group on the aromatic ring. This makes Friedel–Crafts acylation an important way of building molecules during organic synthesis.

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