Electrochemical Cells

01Electrochemical Cells

Setting up half-cells

This section covers assembling metal–metal ion half-cells and preparing the electrodes for reliable EMF measurements.

Metal–metal ion half-cells

A simple half-cell consists of a metal electrode in contact with an aqueous solution containing ions of that metal. Connecting two different half-cells allows their potential difference to be measured.

Suitable combinations can use metals such as zinc, copper, iron or silver with their corresponding soluble metal-ion solutions. A concentration of 1.0moldm31.0\,\mathrm{mol\,dm^{-3}} is commonly used when setting up these cells.

ZnCusalt bridgeVelectron °owZn2+(aq)Cu2+(aq)

Preparing the electrodes

  • Rub each metal strip with sandpaper or emery paper to remove oxide from the surface.
  • Grease can also be removed from the electrode before use.
  • Place each metal in a solution containing its own ions.
  • A long strip can be folded over the edge of the beaker to give a secure point for the crocodile clip.

Half-cells without a metal electrode

If the redox system contains only dissolved species, there is no conducting metal belonging to the redox pair. For example, an FeX2+/FeX3+\ce{Fe^{2+}/Fe^{3+}} half-cell can use an inert platinum electrode. Platinum provides electrical contact but does not take part in the redox reaction.

Exam Tip: A metal–metal ion half-cell needs the metal and a solution containing its ions. If both members of the redox pair are dissolved, state that an inert conducting electrode such as platinum is required.

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