Gas Chromatography

01Gas Chromatography

Gas chromatography phases

This section covers the mobile and stationary phases in gas chromatography and how a sample passes through the apparatus.

Gas chromatography (GC) separates substances by carrying a vaporised sample through a column using a gaseous mobile phase. It can be used with gases, volatile liquids and substances introduced in vapour form.

Phase In gas chromatography
Mobile phase An inert carrier gas, such as helium or nitrogen, transports the sample through the column.
Stationary phase A solid, or a liquid coating held on a solid support. In gas-liquid chromatography the stationary phase is a non-volatile, high-boiling liquid supported on a solid.

The carrier gas is chemically unreactive under the operating conditions, so it can transport the substances being separated without reacting with them.

GC apparatus

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What happens?

  1. The flow of carrier gas is controlled.
  2. The sample is injected and forms a vapour.
  3. The gas stream carries the sample through the column under pressure at high temperature.
  4. The components separate while moving through the stationary phase.
  5. As each component reaches the detector, its response contributes to the chromatogram.

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