Measuring Reaction Rates

01Measuring Reaction Rates

Continuous monitoring

This section covers how a reaction is followed continuously and how gradients from time graphs are used to determine reaction rates.

Following one reaction through time

Continuous monitoring: taking repeated measurements during one reaction so that its progress can be plotted against time.

Required Practical 7 uses both an initial-rate method and a continuous monitoring method. Depending on the reaction, progress can be followed using concentration, gas volume, mass or colour.

Approach What is recorded How it is analysed Example
Continuous monitoring Repeated readings during one run Gradient of a tangent to a graph against time Gas volume or colorimeter readings
Initial-rate clock method Time required to reach the same fixed endpoint Use 1/t1/t as a quantity proportional to initial rate Iodine clock

Reading a time graph

  1. Plot the measured quantity against time and draw an appropriate best-fit curve.
  2. Draw a tangent at the time for which the rate is required.
  3. Calculate Δy/Δx\Delta y/\Delta x for the tangent.

The reaction is fastest where the curve is steepest. As reactants are consumed, the slope becomes less steep; when the measured quantity becomes constant, its gradient is zero.

For a reactant concentration that is decreasing, quote the rate using the magnitude of the negative tangent gradient.

050100150200250300350400450500550600650700750800time / s0.0000.0010.0020.0030.0040.0050.0060.0070.0080.0090.010iodine concentration / mol dm^-3

For the example tangent at 300 s300\ \mathrm{s}:

rate=0.0069580=1.19×105 moldm3s1\text{rate}=\frac{0.0069}{580}=1.19\times10^{-5}\ \mathrm{mol\,dm^{-3}\,s^{-1}}
Exam Tip: If an initial rate is required from continuous data, draw the tangent at t=0t=0. Do not substitute an average gradient from the first few plotted points.

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